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Synthesis of Azadirachtin: A Long but Successful Journey

2007/07/30 by Gemma E. Veitch, Edith Beckmann, Brenda J. Burke +3 · 2 citations
Agricultural and Biological Sciences · Biochemistry, Genetics and Molecular Biology · #Insect Pest Control Strategies #Phytochemical compounds biological activities #Traditional and Medicinal Uses of Annonaceae

paper · doi:10.1002/anie.200703027

openalex publication_date 2007/07/30 · openalex created_date 2025/10/10 · openalex updated_date 2026/07/30

Abstract

22 Years in the making: Azadirachtin (1) was synthesized for the first time by a highly convergent approach, utilizing a Claisen rearrangement and a radical cyclization as key steps. End-game strategies relied on intermediate 2, which could be obtained by synthetic methods as well as by degradation of 1. Bn=benzyl, TBS=tert-butyldimethylsilyl.

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