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The Rietveld method in neutron and X-ray powder diffraction

1982/08/01 by A. Albinati, Alberto Albinati, B. T. M. Willis +1 · 3 citations
Materials Science · Physics and Astronomy · #X-ray Diffraction in Crystallography #Nuclear Physics and Applications #Crystallography and Radiation Phenomena

paper · doi:10.1107/s0021889882012187

Abstract

In the Rietveld method of analysing powder diffraction data, the crystal structure is refined by fitting the entire profile of the diffraction pattern to a calculated profile. There is no intermediate step of extracting structure factors. The method was applied first to diffraction patterns recorded with neutrons at a fixed wavelength. It has now been used successfully for the treatment of results from the four categories of experimental technique, with neutrons or X-rays as the primary radiation and with the scattered intensity measured at a fixed wavelength or at a fixed scattering angle. In this article we discuss the application of the Rietveld method to each of these techniques.

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