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Development of a Semi-Automated System for Routine Preparation of Carbonate Samples

2001/01/01 by N Tisnérat-Laborde, Nadine Tisnérat‐Laborde, Jean-Jacques Poupeau +5 · 1 citation
Earth and Planetary Sciences · Arts and Humanities · Computer Science · #Building materials and conservation #Conservation Techniques and Studies #Seismology and Earthquake Studies

paper · pdf · doi:10.1017/s0033822200038145

Abstract

We constructed a semi-automated system to transform carbonate samples to CO 2 , as a means to increase sample-processing capacity. The physico-chemical process includes hydrolysis of carbonate, quantification of the mass of carbon and CO 2 collection in a glass ampoule. The system is computer-controlled and monitored, and all the data are stored. A single run of five consecutive samples requires about 3.5 hours. Measurements of 14 C concentrations were made on samples of IAEA C-1 Carrara marble to test the reliability of this semi-automated system. These measurements have allowed the determination of the total system background and the memory effect of our system.

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