A nitrogen-gas-stream cryostat for general X-ray diffraction studies
1986/04/01 by J. Cosier, A. M. Glazer · 32 citations
Chemistry · Earth and Planetary Sciences · Materials Science · #Analytical Chemistry (journal) #Chemistry #Chromatography #Composite material #Condensed matter physics #Cryostat #Diffraction #High-pressure geophysics and materials #Inorganic Fluorides and Related Compounds #Liquid nitrogen #Materials science #Nitrogen #Nitrogen gas #Optics #Physics #Range (aeronautics) #Thermodynamics #Volumetric flow rate #X-ray #X-ray Diffraction in Crystallography
paper · doi:10.1107/s0021889886089835
openalex publication_date 1986/04/01 · openalex created_date 2025/10/10 · openalex updated_date 2026/07/31
Abstract
A continuous nitrogen-flow cooling device, generally applicable to X-ray diffraction studies, is described. The device works in the range 77.4 to 323.0 K with a precision of ±0.1 K and a liquid-nitrogen constant consumption rate of 0.5 l h−1 over the whole temperature range. The supply vessel is unpressurized, so that refilling can be done without any observable influence on the cooling of the sample.
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