1992/07/15 by G. Ferguson, John F. Gallagher, Damien M. Murphy +3 · 2 citations
Chemistry · Environmental Science · #Crystal structures of chemical compounds #Thallium and Germanium Studies #Organometallic Compounds Synthesis and Characterization
paper · pdf · doi:10.1107/s0108270191015056
openalex publication_date 1992/07/15 · openalex created_date 2025/10/10 · openalex updated_date 2026/07/19
, b = 19.974 (7), c = 23.264 (11) A, a = 107.78 (4), 13 = 1.03.54 (4), y= 101.51 (3) , V = 6338 (5)/~3, Z = 16, Dx = 1.34 g cm -3, a(Mo Ka) = 0.71073A, /z = 19.1cm-1, F(000)=2624, T= 293 K, R = 0.055 for 6846 observed reflections. The eight independent molecules in the asymmetric unit form two independent O--H...O hydrogen-bonded tetramers with the O atoms in a flattened tetrahedral arrangement [hydrogen-bond distances in the range 2.609 (11) to 2.657 (11)A]. The Ge atoms are tetrahedrally coordinated with mean Gc O 1.791 (7) and Gc C 1.931 (8) A.