2026/03/28 by T. Ben Britton, M. Haroon Qaiser, Ruth M. Birch · 1 voice
Physics and Astronomy · #cond-mat.mtrl-sci
paper · pdf · doi:10.1016/j.ultramic.2026.114384
arxiv published 2026/03/28 · arxiv updated 2026/04/24
Scanning electron microscopy combined with electron backscatter diffraction (EBSD) and electron channeling provides rich crystallographic contrast, but the mutual influence of channeling-in and channeling-out is often simplified or neglected in quantitative analyses. In this work, we use selected-area electron channeling patterns (SA-ECPs) acquired from a single-crystal silicon wafer while recording an EBSD pattern at every incident beam direction, thereby directly probing how channeling-in affects the EBSD signal. We show that common Hough-based quality metrics (pattern quality, band contrast, and band slope), pattern-matching cross-correlation coefficients, and Fourier-based signal-to-noise ratios all exhibit strong crystallographic modulations that follow the underlying ECP, in both raw and background-corrected patterns. Similar wide-angle channeling features are also visible in conventional, low-magnification EBSD maps, indicating that channeling-in effects are relevant under routine mapping conditions and not only in specialized ECP experiments. These observations highlight that channeling-in can significantly bias quality-based interpretation of EBSD data, with consequences for methods such as pattern blurring analysis, high-resolution strain mapping, and emerging statistical or machine-learning approaches that rely on subtle variations in diffraction patterns. The combined SA-ECP and EBSD strategy presented here offers a practical framework to visualize and potentially control channeling-in/channeling-out coupling in the SEM, suggesting new routes to design experiments and detector configurations that either mitigate or intentionally exploit these dynamical effects.