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Characterization of nanoparticles prepared by acid hydrolysis of various starches

2012/01/19 by Hee‐Young Kim, Ju Hun Lee, Jong‐Yea Kim +3 · 1 citation
Agricultural and Biological Sciences · Nursing · #Food and Agricultural Sciences #Food composition and properties #Proteins in Food Systems

paper · doi:10.1002/star.201100105

crossref issued 2012/01/19 · crossref published 2012/01/19 · crossref published-online 2012/01/19 · openalex publication_date 2012/01/19 · crossref created 2012/01/19 · crossref published-print 2012/05/01 · crossref deposited 2023/10/07 · openalex created_date 2025/10/10 · crossref indexed 2026/08/03 · openalex updated_date 2026/08/04

Abstract

Abstract Various starches of different AM contents and origins such as wx maize, normal maize, high AM maize, potato, and mungbean starches were hydrolyzed using a H 2 SO 4 solution (3.16 M) at 40°C for 7 days, and the starch particles were isolated from the hydrolysates by centrifugation. The hydrolysis rates varied from 61.4 to 90.9% depending on the starch type. Unexpectedly, A‐type starches were more resistant to the acid hydrolysis than B‐type starches. XRD results revealed that the starch particles with B‐crystalline type exhibited a decrease in peak intensity. In addition, in a DSC analysis, the crystals remaining in the B‐type starch particles were readily disrupted in the water dispersion so that no melting endotherm appeared. Electron microscopy confirmed that the starch particles had round or oval shapes with diameters ranging from 40 to 70 nm, which possibly represented the starch blocklets in granules. The acid degraded mainly AM and long AP chains, resulting in increasing the proportion of short chains.

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