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Bernardite, a new thallium arsenic sulphosalt from Allchar, Macedonia, with a determination of the crystal structure

1989/12/01 by J. Pašava, Jan Pašava, F. Pertlik +2
Materials Science · #Crystal Structures and Properties #Glass properties and applications #Solid-state spectroscopy and crystallography

paper · doi:10.1180/minmag.1989.053.373.03

crossref issued 1989/12/01 · crossref published 1989/12/01 · crossref published-print 1989/12/01 · openalex publication_date 1989/12/01 · crossref created 2006/12/07 · crossref published-online 2018/07/05 · crossref deposited 2021/02/04 · openalex created_date 2025/10/10 · crossref indexed 2026/07/30 · openalex updated_date 2026/07/31

Abstract

Abstract The new mineral bernardite has been identified on one specimen from Allchar, Macedonia, Yugoslavia, together with orpiment and realgar. It forms black crystals, the size of which may exceed 1 mm. The streak is deep red; on an arbitrarily oriented section R (589nm) ranges from 23.8 to 24.7% in air, from 10.2 to 11.6% in oil. Microprobe analyses together with an X-ray structure analysis suggest the ideal formula TlAs 5 S 8 , with a possible replacement of As by Sb up to 15 wt. %. Monoclinic; a 15.647(4), b 8.038(3), c 10.750(3) Å, β 91.27(3)°; space group P 2 1 / c ; Z = 4; R = 0.049, w R = 0.036 for 2410 reflections. The atomic arrangement consists of a 3-dimensional As 5 S 8 framework with eight-coordinated T1 in its holes. The mineral is named for Doc. Dr Jan H. Bernard, Prague, Czechoslovakia.

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