2024/03/13 by Joseph S. Elias · 1 voice
Chemical Engineering · Chemistry · Engineering · #Analytical Chemistry and Sensors #Electrochemical Analysis and Applications #Electrochemical sensors and biosensors
paper · pdf · doi:10.1021/acs.jchemed.3c01044
openalex publication_date 2024/03/13 · openalex created_date 2025/10/10 · openalex updated_date 2026/06/14
High Resolution Image Download MS PowerPoint Slide We report the design of a low-cost electrochemical workstation and open-source graphical user interface capable of performing a variety of electrochemical methods in an undergraduate teaching laboratory. The instrument─based on the popular Arduino microcontroller board─can be constructed from common components for 40 USD. The modular design of the instrument enables instructors to employ it to fit the needs of their curricula and allows for the acquisition of potentiostatic and galvanostatic data. The incorporation of positive-feedback ohmic drop compensation into the hardware, coupled with the judicious use of signal-averaging within the user-friendly LabVIEW standalone program, allow us to acquire meaningful quantitative electrochemical data (e.g., Tafel slopes) comparable to much more expensive research-grade potentiostats. The companion program is available free of charge online and vastly improves the scope of electrochemical methods available to undergraduate laboratories. We demonstrate the versatility of this potentiostat/galvanostat by employing it in General Chemistry and Inorganic Chemistry courses in modules that touch on sustainability, renewable energy, and electrocatalysis. We hope these improvements will enable instructors to incorporate electroanalytical techniques into their undergraduate curricula and empower the next generation of scientists to take full advantage of these methods in their research.