2003/04/28 by Peter J. Chupas, Xiangyun Qiu, Chupas, Peter J. +9 · 1 citation
Physics and Astronomy · #Condensed Matter (cond-mat) #FOS: Physical sciences #cond-mat
paper · pdf · doi:10.48550/arxiv.cond-mat/0304638
5 pages, 4 figures, submitted to J. Appl. Cryst
arxiv created 2003/04/28 · arxiv updated 2009/11/30
An image plate (IP) detector coupled with high energy synchrotron radiation was used for atomic pair distribution function (PDF) analysis, with high probed momentum transfer \Qmax ≤ 28.5 \RAA from crystalline materials. Materials with different structural complexities were measured to test the validity of the quantitative data analysis. Experimental results are presented here for crystalline Ni, crystalline \alf, and the layered Aurivillius type oxides \bivo and \bivtio . Overall, the diffraction patterns show good counting statistics with measuring time from one to tens of seconds. The PDFs obtained are of high quality. Structures may be refined from these PDFs, and the structural models are consistent with the published literature. Data sets from similar samples are highly reproducible.